tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate

Base Information

• Chemical Name: tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate
• CAS No.: 912368-78-6
• Molecular Formula: C₁₉H₂₈N₂O₅
• Molecular Weight: 364.442

Synonyms:tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate

Chemical Property of tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

(S)-Benzyltert-butyl(5-oxohexane-1,4-diyl)dicarbamate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate

There total 1 articles about tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

Boc-Orn(Z)-OH (2480-93-5) + methyllithium (917-54-4) → tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate (912368-78-6)

Guidance literature:

In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 5.33333h;

DOI:10.1021/acs.jmedchem.7b01490

Reference yield: 100.0%

tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate (912368-78-6) → tert-butyl 2-methylpiperidin-3-ylcarbamate (1150618-42-0,1791402-58-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 72h; under 760.051 Torr; Pressure;

DOI:10.1021/acs.jmedchem.7b01490

Reference yield: 100.0%

tert-butyl ((1S)-1-acetyl-4-{[(benzyloxy)carbonyl]amino}butyl)carbamate (912368-78-6) → tert-butyl [trans-2-methylpiperidin-3-yl]carbamate (1791402-58-8)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; for 72h; under 760.051 Torr;

upstream raw materials:

Boc-Orn(Z)-OH

methyllithium

Downstream raw materials:

tert-butyl [trans-2-methylpiperidin-3-yl]carbamate

tert-Butyl [(3R)-2-methylpiperidin-3-yl]carbamate

tert-butyl 2-methylpiperidin-3-ylcarbamate

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