O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

Base Information

Chemical Name:O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate
CAS No.:1025913-33-0
Molecular Formula:C₂₂H₂₉N₅OS
Molecular Weight:411.571
Hs Code.:

Synonyms:O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

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Chemical Property of O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

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Technology Process of O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

There total 1 articles about O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 16420-13-6
N,N-Dimethylthiocarbamoyl chloride

: (2-hydroxyphenyl)bis(3-isopropylpyrazolyl)methane

: 1025913-33-0
O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 3h; Heating;
DOI:10.1002/1099-0690(200211)2002:21<3632::AID-EJOC3632>3.0.CO;2-2

Reference yield: 70.0%

: 1025913-33-0
O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

: 1026902-33-9
S-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

Guidance literature:: at 580 ℃; under 0.1 Torr;
DOI:10.1002/1099-0690(200211)2002:21<3632::AID-EJOC3632>3.0.CO;2-2

Reference yield:

: 1025913-33-0
O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

: 1027064-65-8
1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 580 °C / 0.1 Torr

2: 80 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 46 percent / NaH / tetrahydrofuran / 0.42 h / Heating

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1002/1099-0690(200211)2002:21<3632::AID-EJOC3632>3.0.CO;2-2