1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Base Information

Chemical Name:1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane
CAS No.:1027064-65-8
Molecular Formula:C₂₁H₂₇BrN₄S
Molecular Weight:447.442
Hs Code.:

Synonyms:1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Suppliers and Price of 1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

There total 4 articles about 1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 106-93-4
ethylene dibromide

: 2-[bis(3'-isopropylpyrazol-1'-yl)methyl]benzenethiol

: 1027064-65-8
1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 0.416667h; Heating;
DOI:10.1002/1099-0690(200211)2002:21<3632::AID-EJOC3632>3.0.CO;2-2

Reference yield:

: (2-hydroxyphenyl)bis(3-isopropylpyrazolyl)methane

: 1027064-65-8
1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / NaH / tetrahydrofuran / 3 h / Heating

2: 70 percent / 580 °C / 0.1 Torr

3: 80 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

4: 46 percent / NaH / tetrahydrofuran / 0.42 h / Heating

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1002/1099-0690(200211)2002:21<3632::AID-EJOC3632>3.0.CO;2-2

Reference yield:

: 1025913-33-0
O-{2-[bis(3'-isopropylpyrazol-1'-yl)methyl]phenyl}-N,N-dimethylthiocarbamate

: 1027064-65-8
1-{2'-[bis(3-isopropylpyrazol-1-yl)methyl]phenylsulfanyl}-2-bromoethane

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 580 °C / 0.1 Torr

2: 80 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 46 percent / NaH / tetrahydrofuran / 0.42 h / Heating

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1002/1099-0690(200211)2002:21<3632::AID-EJOC3632>3.0.CO;2-2