Technology Process of 2,6-Di-n-butyl-3,5-diethyl-2,3,5,6-tetrahydro-4H-1,3,5,2,6-thiadiazadiborin-4-thion
There total 1 articles about 2,6-Di-n-butyl-3,5-diethyl-2,3,5,6-tetrahydro-4H-1,3,5,2,6-thiadiazadiborin-4-thion which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
n-butyllithium;
In
hexane; Petroleum ether;
byproducts: butane, LiBr; the urea in petroleum ether was refluxed under N2 with n-BuLi in hexanefor 48 h; the solvents were removed in vac., the residue was fractional distd.; elem. anal.;