5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

Base Information

Chemical Name:5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid
CAS No.:370097-77-1
Molecular Formula:C₂₄H₃₂O₆
Molecular Weight:416.514
Hs Code.:

Synonyms:5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

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Chemical Property of 5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

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Technology Process of 5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

There total 5 articles about 5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 370097-74-8
2,2-bis[3-(4-methoxybenzyloxy)-1-propyl]malonic acid

: 370097-77-1
5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

Guidance literature:: In 1,2-dichloro-benzene; at 150 ℃; for 0.666667h;
DOI:10.1021/jo0101508

Reference yield:

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 370097-77-1
5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 10-camphorsulfonic acid / cyclohexane; CH₂Cl₂ / 12 h / 20 °C

2: 64 percent / NaH; Bu₄NI / tetrahydrofuran / 48 h / Heating

3: 65 percent / KOH / ethanol; H₂O / 8 h / 80 °C

4: 85 percent / 1,2-dichloro-benzene / 0.67 h / 150 °C

With potassium hydroxide; (1S)-10-camphorsulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane; cyclohexane; water; 1,2-dichloro-benzene;
DOI:10.1021/jo0101508

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 370097-77-1
5-(4-methoxybenzyloxy)-2-[3-(4-methoxybenzyloxy)-1-propyl]pentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: NaH / diethyl ether / 4 h / 0 - 20 °C

2: 10-camphorsulfonic acid / cyclohexane; CH₂Cl₂ / 12 h / 20 °C

3: 64 percent / NaH; Bu₄NI / tetrahydrofuran / 48 h / Heating

4: 65 percent / KOH / ethanol; H₂O / 8 h / 80 °C

5: 85 percent / 1,2-dichloro-benzene / 0.67 h / 150 °C

With potassium hydroxide; (1S)-10-camphorsulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; cyclohexane; water; 1,2-dichloro-benzene;
DOI:10.1021/jo0101508