4-butylphenyl dimethylsulfamate

Base Information

Chemical Name:4-butylphenyl dimethylsulfamate
CAS No.:1501945-39-6
Molecular Formula:C₁₂H₁₉NO₃S
Molecular Weight:257.354
Hs Code.:

Synonyms:4-butylphenyl dimethylsulfamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-butylphenyl dimethylsulfamate

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Technology Process of 4-butylphenyl dimethylsulfamate

There total 1 articles about 4-butylphenyl dimethylsulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1638-22-8
4-n-butylphenol

: 13360-57-1
dimethylamino sulfonyl chloride

: 1501945-39-6
4-butylphenyl dimethylsulfamate

Guidance literature:: 4-n-butylphenol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere;

dimethylamino sulfonyl chloride; In tetrahydrofuran; mineral oil; at 0 - 24 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol403209k

Reference yield: 94.0%

: 4518-10-9
Methyl 3-aminobenzoate

: 1501945-39-6
4-butylphenyl dimethylsulfamate

: 1501945-35-2
methyl 3-((4-butylphenyl)amino)benzoate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; cis-[1,1'-bis(diphenylphosphino)ferrocene](2-methylphenyl)nickel(II) chloride; acetonitrile; at 110 ℃; for 16h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol403209k