C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾
CAS No.:1415578-07-2
Molecular Formula:C₁₆H₁₆F₅O₄S₂*Na
Molecular Weight:454.414
Hs Code.:

C<sub>16</sub>H<sub>16</sub>F<sub>5</sub>O<sub>4</sub>S<sub>2</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

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Chemical Property of C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

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Technology Process of C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

There total 4 articles about C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415578-06-1
C₁₂H₁₃F₅OS₂

: 108-59-8
malonic acid dimethyl ester

: 1415578-07-2
C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

Guidance literature:: malonic acid dimethyl ester; With sodium methylate; In tetrahydrofuran; methanol; for 0.25h; Reflux;

C₁₂H₁₃F₅OS₂; In tetrahydrofuran; methanol; for 0.5h; Reflux;

Reference yield:

: 1415578-04-9
C₉H₉F₅OS₂

: 1415578-07-2
C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloroform / 8 h / 0 °C

2.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

2.2: 0.5 h / Reflux

With sodium methylate; In tetrahydrofuran; methanol; chloroform; 1.1: |Wittig Olefination;

Reference yield:

: 2993-24-0
4-(pentafluorosulfanyl)aniline

: 1415578-07-2
C₁₆H₁₆F₅O₄S₂^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; sulfuric acid; sodium nitrite / water / 0.17 h / 0 °C

1.2: 0.5 h / 60 °C

1.3: 1 h / 0 - 30 °C / Inert atmosphere

2.1: triethylamine / tetrahydrofuran / 2 h / 0 °C / Cooling with ice

3.1: chloroform / 8 h / 0 °C

4.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

4.2: 0.5 h / Reflux

With sulfuric acid; sodium methylate; acetic acid; triethylamine; sodium nitrite; In tetrahydrofuran; methanol; chloroform; water; 3.1: |Wittig Olefination;