[2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

Base Information

Chemical Name:[2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol
CAS No.:875109-02-7
Molecular Formula:C₄₉H₅₀O₇
Molecular Weight:750.932
Hs Code.:

Synonyms:[2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

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Chemical Property of [2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

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Technology Process of [2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

There total 6 articles about [2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 875109-00-5
2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)benzaldehyde

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 875109-02-7
[2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

Guidance literature:: 2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)benzaldehyde; 4-methoxyphenyl magnesium bromide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 13h;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmc.2011.08.005

Reference yield: 74.0%

: 875109-02-7
[2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

Guidance literature:

Reference yield:

: 875108-95-5
2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-gluco-pyranosyl)benzoic acid methyl ester

: 875109-02-7
[2-(2,3,4,6-tetra-O-benzyl-5a-carba-β-D-glucopyranosyl)phenyl]-4-methoxyphenylmethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 55 °C

1.2: 20 °C

2.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C

3.1: tetrahydrofuran; diethyl ether / 13 h / 20 °C

With lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2011.08.005