methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

Base Information

Chemical Name:methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate
CAS No.:114250-26-9
Molecular Formula:C₂₈H₃₀O₅
Molecular Weight:446.543
Hs Code.:

Synonyms:methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

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Chemical Property of methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

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Technology Process of methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

There total 5 articles about methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 616-38-6
carbonic acid dimethyl ester

: 114250-17-8
1-<4-(1,1-dimethylethyl)-2,5-bis(phenylmethoxy)phenyl>ethanone

: 114250-26-9
methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

Guidance literature:: With sodium hydride; Heating;
DOI:10.1021/jm00402a032

Reference yield:

: 35292-10-5
2-(1,1-dimethylethyl)-1,4-bis(phenylmethoxy)benzene

: 114250-26-9
methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / N-bromosuccinimde / dimethylformamide / 24 h / Ambient temperature

2: 1.) Mg, I₂ / 1) THF, reflux; 2) THF, -78 --> room temperature, overnight

3: 91 percent / NaH / Heating

With N-Bromosuccinimide; iodine; sodium hydride; magnesium; In N,N-dimethyl-formamide;
DOI:10.1021/jm00402a032

Reference yield:

: 100-39-0
benzyl bromide

: 114250-26-9
methyl 4-(1,1-dimethylethyl)-β-oxo-2,5-bis(phenylmethoxy)benzenepropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / K₂CO₃ / acetone / 72 h / Heating

2: 95 percent / N-bromosuccinimde / dimethylformamide / 24 h / Ambient temperature

3: 1.) Mg, I₂ / 1) THF, reflux; 2) THF, -78 --> room temperature, overnight

4: 91 percent / NaH / Heating

With N-Bromosuccinimide; iodine; sodium hydride; potassium carbonate; magnesium; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00402a032