(E)-methyl dec-2-en-1-yl(tosyl)carbamate

Base Information

Chemical Name:(E)-methyl dec-2-en-1-yl(tosyl)carbamate
CAS No.:1012367-21-3
Molecular Formula:C₁₉H₂₉NO₄S
Molecular Weight:367.51
Hs Code.:

Synonyms:(E)-methyl dec-2-en-1-yl(tosyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-methyl dec-2-en-1-yl(tosyl)carbamate

Chemical Property:

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Technology Process of (E)-methyl dec-2-en-1-yl(tosyl)carbamate

There total 3 articles about (E)-methyl dec-2-en-1-yl(tosyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 872-05-9,17438-89-0,25189-70-2
1-Decene

: 14437-03-7
methyl tosylcarbamate

: methyl 2-tosyl-3-vinyldecanoate

: 1012367-21-3
(E)-methyl dec-2-en-1-yl(tosyl)carbamate

Guidance literature:: With air; [1,2-bis-(phenylsulfinyl)ethane]palladium(II) acetate; tetrabutylammonium acetate; p-benzoquinone; In tert-butyl methyl ether; at 45 ℃; for 72h; optical yield given as %de; chemoselective reaction;
DOI:10.1021/ja903939k

Reference yield:

: 872-05-9,17438-89-0,25189-70-2
1-Decene

: 14437-03-7
methyl tosylcarbamate

: methyl 2-tosyl-3-vinyldecanoate

: (Z)-methyl dec-2-en-1-yl(tosyl)carbamate

: 1012367-21-3
(E)-methyl dec-2-en-1-yl(tosyl)carbamate

Guidance literature:: With p-benzoquinone; Pd[1,2-bis(phenylsulfinyl)ethane](OAc)2; (+)-(S,S)-Cr(salen)Cl; In various solvent(s); at 45 ℃; for 72h;
DOI:10.1021/ja710206u

Reference yield:

: 56991-23-2
dec-1-en-3-yl acetate

: 14437-03-7
methyl tosylcarbamate

: 2497-23-6
(E)-2-decenyl acetate

: methyl 2-tosyl-3-vinyldecanoate

: (Z)-methyl dec-2-en-1-yl(tosyl)carbamate

: 1012367-21-3
(E)-methyl dec-2-en-1-yl(tosyl)carbamate

Guidance literature:: With p-benzoquinone; (+)-(S,S)-Cr(salen)Cl; In various solvent(s); at 45 ℃; for 72h; Further Variations:; Reagents; Product distribution;
DOI:10.1021/ja710206u