N-methyl-N-cyclohexyl cyanamide

Base Information

• Chemical Name: N-methyl-N-cyclohexyl cyanamide
• CAS No.: 49677-01-2
• Molecular Formula: C₈H₁₄N₂
• Molecular Weight: 138.213

Synonyms:N-methyl-N-cyclohexyl cyanamide

Chemical Property of N-methyl-N-cyclohexyl cyanamide

Chemical Property:

Purity/Quality:

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Technology Process of N-methyl-N-cyclohexyl cyanamide

There total 5 articles about N-methyl-N-cyclohexyl cyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N-methylcyclohexylamine (100-60-7) + bromocyane (506-68-3) → N-methyl-N-cyclohexyl cyanamide (49677-01-2)

Guidance literature:

In tetrahydrofuran; diethyl ether; at 0 ℃; for 3h;

DOI:10.1002/adsc.201500637

Reference yield: 83.0%

N-methylcyclohexylamine (100-60-7) + 3-oxo-1λ3-benzo[d][1,2]iodaoxole-1(3H)-carbonitrile (172876-96-9) → N-methyl-N-cyclohexyl cyanamide (49677-01-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 0.166667h;

DOI:10.1016/j.tetlet.2021.153564

Reference yield: 75.0%

2-(N-cyclohexyl-N-methylamino)acetamide → N-methyl-N-cyclohexyl cyanamide (49677-01-2)

Guidance literature:

With tetraethylammonium bromide; In acetonitrile; at 60 ℃; for 0.416667h;

DOI:10.1055/s-2007-991093

upstream raw materials:

N-methylcyclohexylamine

bromocyane

3-oxo-1λ³-benzo[d][1,2]iodaoxole-1(3H)-carbonitrile

Downstream raw materials:

antimony pentachloride-cyclohexylmethylcyanamide

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