1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

Base Information

Chemical Name:1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene
CAS No.:95113-19-2
Molecular Formula:C₂₆H₄₀O₂S₂
Molecular Weight:448.734
Hs Code.:

Synonyms:1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

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Chemical Property of 1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

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Technology Process of 1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

There total 3 articles about 1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 75-66-1
2-methylpropan-2-thiol

: 95113-17-0,95113-18-1
(E)-3-tert-Butyl-1-tert-butylsulfanyl-5-(2-dimethoxymethyl-phenyl)-pent-1-en-4-yn-3-ol

: 95113-19-2
1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

Guidance literature:: With trifluoroacetic acid; trimethyl orthoformate; In dichloromethane; at -15 ℃; for 1h;
DOI:10.1246/cl.1984.2001

Reference yield:

: 73624-71-2
(E)-1-tert-Butylsulfanyl-4,4-dimethyl-pent-1-en-3-one

: 95113-19-2
1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent

2: 60 percent / CF₃CO₂H, CH(OCH₃)3 / CH₂Cl₂ / 1 h / -15 °C

With trifluoroacetic acid; trimethyl orthoformate; In dichloromethane;
DOI:10.1246/cl.1984.2001

Reference yield:

: 95113-16-9
C₁₁H₁₁LiO₂

: 95113-19-2
1-((Z)-3-tert-Butyl-5,5-bis-tert-butylsulfanyl-pent-3-en-1-ynyl)-2-dimethoxymethyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent

2: 60 percent / CF₃CO₂H, CH(OCH₃)3 / CH₂Cl₂ / 1 h / -15 °C

With trifluoroacetic acid; trimethyl orthoformate; In dichloromethane;
DOI:10.1246/cl.1984.2001