1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol

Base Information

• Chemical Name: 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol
• CAS No.: 249757-75-3
• Molecular Formula: C₂₉H₃₂O₄
• Molecular Weight: 444.571

Synonyms:1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol

Chemical Property of 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol

Chemical Property:

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Technology Process of 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol

There total 2 articles about 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) + (2S,3S,4R)-2-(1-Hydroxy-1-methyl-ethyl)-3,4-dihydro-2H-pyran-3,4-diol → 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol (249757-75-3)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo010880f

Reference yield:

C8H14O4 (249757-73-1) + benzyl bromide (100-39-0) → 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol (249757-75-3)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; sodium hydride; In dimethyl sulfoxide;

DOI:10.1021/ol990188v

Reference yield:

C43H52O9 (249757-79-7) + 1,5-anhydro-2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-D-arabino-hept-1-enitol (249757-75-3) → C72H84O13

Guidance literature:

With triphenylphosphine hydrobromide; In dichloromethane; at 20 ℃;

DOI:10.1021/ol990188v

upstream raw materials:

benzyl bromide

C₈H₁₄O₄

Downstream raw materials:

(2S)-[[2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-α-D-arabino-heptopyranosyl]oxy]propanoic acid ethyl ester

C₆₅H₇₈O₁₂

C₆₃H₇₄O₁₂

(2S)-2-[[2,7-dideoxy-6-C-methyl-3,4,6-tris-O-(phenylmethyl)-α-D-arabino-heptopyranosyl]oxy]propanoic acid

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