4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate)

Base Information

• Chemical Name: 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate)
• CAS No.: 131169-39-6
• Molecular Formula: C₂₈H₃₄O₆S₂
• Molecular Weight: 530.706
• Mol file: 131169-39-6.mol

Synonyms:4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate)

Chemical Property of 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate)

There total 1 articles about 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4-[4-(4-hydroxybutyl)phenyl]butan-1-ol (21240-37-9) + p-toluenesulfonyl chloride (98-59-9) → 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate) (131169-39-6)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1002/cmdc.201000097

Reference yield: 59.0%

5-hydroxyethyl-4-methylthiazole (137-00-8,8042-97-5) + 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate) (131169-39-6) → 5-(2-hydroxyethyl)-3-[4-(4-{4-[5-(2-hydroxyethyl)thiazol-3-ium-3-yl]butyl}phenyl)butyl]-4-methylthiazol-3-ium chloride

Guidance literature:

5-hydroxyethyl-4-methylthiazole; 4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate); In acetonitrile; at 150 ℃; for 1h; Microwave irradiation;

With Dowex resin (Cl^- form); In water;

DOI:10.1002/cmdc.201000097

Reference yield: 51.0%

4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate) (131169-39-6) + 4‐methyl‐5‐(2‐methoxyethyl)thiazole (98316-89-3) → 3,3'-[4,4'-(1,4-phenylene)bis(butane-4,1-diyl)]bis[5-(2-methoxyethyl)-4-methylthiazol-3-ium] chloride

Guidance literature:

4,4'-(1,4-phenylene)bis(butane-4,1-diyl)bis(4-methylbenzene sulfonate); 4‐methyl‐5‐(2‐methoxyethyl)thiazole; In acetonitrile; at 150 ℃; for 1h; Microwave irradiation;

With Dowex resin (Cl^- form); In water;

DOI:10.1002/cmdc.201000097

upstream raw materials:

4-[4-(4-hydroxybutyl)phenyl]butan-1-ol

p-toluenesulfonyl chloride

Downstream raw materials:

C₃₀H₅₈N₈