Technology Process of C6H11NO5*C9H12N4
There total 5 articles about C6H11NO5*C9H12N4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Candida antarctica lipase B; triethylamine;
In
di-isopropyl ether;
at 45 ℃;
for 6h;
Enzymatic reaction;
DOI:10.1016/j.tetlet.2014.06.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / tetrahydrofuran
2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran
3.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 20 °C
3.2: 80 °C
4.1: trifluoroacetic acid / dichloromethane / 20 °C
5.1: triethylamine; Candida antarctica lipase B / di-isopropyl ether / 6 h / 45 °C / Enzymatic reaction
With
Candida antarctica lipase B; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 9-bora-bicyclo[3.3.1]nonane; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; di-isopropyl ether; toluene;
DOI:10.1016/j.tetlet.2014.06.027
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 20 °C
1.2: 80 °C
2.1: trifluoroacetic acid / dichloromethane / 20 °C
3.1: triethylamine; Candida antarctica lipase B / di-isopropyl ether / 6 h / 45 °C / Enzymatic reaction
With
Candida antarctica lipase B; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; trifluoroacetic acid;
In
dichloromethane; di-isopropyl ether; toluene;
DOI:10.1016/j.tetlet.2014.06.027
