methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

Base Information

Chemical Name:methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate
CAS No.:1616290-33-5
Molecular Formula:C₂₁H₂₈N₂O₅
Molecular Weight:388.464
Hs Code.:

Synonyms:methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

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Chemical Property of methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

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Technology Process of methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

There total 9 articles about methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 1173081-96-3
(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methylamine hydrochloride

: 1616290-31-3
methyl 3-(propan-2-yloxy)-2-(prop-2-en-1-yloxy)benzoate

: 1616290-33-5
methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

Guidance literature:: methyl 3-(propan-2-yloxy)-2-(prop-2-en-1-yloxy)benzoate; With dimethylsulfide; ozone; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methylamine hydrochloride; In methanol; at 20 ℃; for 0.0833333h;

With sodium cyanoborohydride; In methanol; at 20 ℃; for 14.5h;

Reference yield:

: 277312-95-5
8-hydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

: 1616290-33-5
methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.08 h / 20 °C

1.2: 1.33 h / 20 °C

2.1: methanol / 3.66 h

3.1: caesium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

4.1: dimethylsulfide; ozone / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.2: 0.08 h / 20 °C

4.3: 14.5 h / 20 °C

With dimethylsulfide; caesium carbonate; ozone; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1616290-29-9
2,2-dimethyl-8-(propan-2-yloxy)-4H-1,3-benzodioxin-4-one

: 1616290-33-5
methyl 2-(2-{[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]amino}ethoxy)-3-(propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 3.66 h

2.1: caesium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C

3.1: dimethylsulfide; ozone / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.2: 0.08 h / 20 °C

3.3: 14.5 h / 20 °C

With dimethylsulfide; caesium carbonate; ozone; In methanol; dichloromethane; N,N-dimethyl-formamide;