Benzoic acid, 2-hydroxy-3-(1-methylethoxy)-, methyl ester

Base Information

Chemical Name:Benzoic acid, 2-hydroxy-3-(1-methylethoxy)-, methyl ester
CAS No.:193882-86-9
Molecular Formula:C11H14O4
Molecular Weight:210.23
Hs Code.:
Mol file:193882-86-9.mol

Synonyms:methyl 3-(1-methylethoxy)salicylate;2-Hydroxy-3-isopropoxy-benzoic acid methyl ester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2-hydroxy-3-(1-methylethoxy)-, methyl ester

Chemical Property:

PSA：55.76000
LogP:1.96600

Purity/Quality:

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Technology Process of Benzoic acid, 2-hydroxy-3-(1-methylethoxy)-, methyl ester

There total 4 articles about Benzoic acid, 2-hydroxy-3-(1-methylethoxy)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1616290-29-9
2,2-dimethyl-8-(propan-2-yloxy)-4H-1,3-benzodioxin-4-one

: 124-41-4
sodium methylate

: 193882-86-9
methyl 2-hydroxy-3-(propan-2-yloxy)benzoate

Guidance literature:: In methanol; for 3.66h;

Reference yield: 56.0%

: 75-30-9
2-iodo-propane

: 2411-83-8
methyl-2,3-dihydroxybenzoate

: 193882-86-9
methyl 2-hydroxy-3-(propan-2-yloxy)benzoate

Guidance literature:: With potassium carbonate; In acetone; at 85 ℃; for 18h;
DOI:10.1016/S0223-5234(97)81676-5

Reference yield:

: 303-38-8
2,3-Dihydroxybenzoic acid

: 193882-86-9
methyl 2-hydroxy-3-(propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / trifluoroacetic anhydride / 16.95 h / -5 - 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.08 h / 20 °C

2.2: 1.33 h / 20 °C

3.1: methanol / 3.66 h

With caesium carbonate; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide; trifluoroacetic anhydride;