Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

Base Information

Chemical Name:Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine
CAS No.:274917-46-3
Molecular Formula:C₃₅H₂₈N₂
Molecular Weight:476.621
Hs Code.:

Synonyms:Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

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Chemical Property of Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

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Technology Process of Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

There total 6 articles about Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 525-06-4
diphenyl ketene

: C₂₄H₂₇N₂P

: 274917-46-3
Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

Guidance literature:: In toluene; at 25 ℃; for 1h;
DOI:10.1021/jo991826q

Reference yield:

: 13209-38-6
(2-aminophenyl)(phenyl)methanol

: 274917-46-3
Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaNO₂; 6N HCl / H₂O / 0.5 h / 0 °C

1.2: 60 percent / NaN₃ / H₂O / 4 h / 20 °C

2.1: 75 percent / diethyl azodicarboxylate; triphenylphosphane / tetrahydrofuran / 25 h / 0 - 20 °C

3.1: 91 percent / hydrazine hydrate / tetrahydrofuran; ethanol / 8 h / Heating

4.1: MgSO₄ / diethyl ether / 12 h / 25 °C

5.1: toluene / 20 °C

6.1: toluene / 1 h / 25 °C

With hydrogenchloride; magnesium sulfate; hydrazine hydrate; triphenylphosphine; sodium nitrite; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; ethanol; water; toluene; 1.1: Diazotization / 1.2: Substitution / 2.1: Condensation / 3.1: Elimination / 4.1: Condensation / 5.1: Addition / 6.1: Addition;
DOI:10.1021/jo991826q

Reference yield:

: 274917-70-3
2-azido-α-phenylbenzyl alcohol

: 274917-46-3
Diphenylvinylidene-[2-(phenyl-{[1-p-tolyl-meth-(E)-ylidene]-amino}-methyl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / diethyl azodicarboxylate; triphenylphosphane / tetrahydrofuran / 25 h / 0 - 20 °C

2: 91 percent / hydrazine hydrate / tetrahydrofuran; ethanol / 8 h / Heating

3: MgSO₄ / diethyl ether / 12 h / 25 °C

4: toluene / 20 °C

5: toluene / 1 h / 25 °C

With magnesium sulfate; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; ethanol; toluene; 1: Condensation / 2: Elimination / 3: Condensation / 4: Addition / 5: Addition;
DOI:10.1021/jo991826q