P_TM₈₇

Base Information

Chemical Name:P_TM₈₇
CAS No.:1189395-15-0
Molecular Formula:C₃₃H₃₆N₂O₂
Molecular Weight:492.661
Hs Code.:

Synonyms:P_TM₈₇

Suppliers and Price of P_TM₈₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of P_TM₈₇

Chemical Property:

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Technology Process of P_TM₈₇

There total 3 articles about P_TM₈₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1189395-12-7
1-(4-tert-butyl-benzyl)-4-[4-(1,4-dimethoxy-3-methyl-naphthalen-2-ylmethyl)-phenyl]-piperazine

: 1189395-15-0
P_TM₈₇

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃;

Reference yield:

: 1189395-10-5
2-(4-chloro-benzyl)-1,4-dimethoxy-3-methyl-naphthalene

: 1189395-15-0
P_TM₈₇

Guidance literature:: Multi-step reaction with 2 steps

1: sodium t-butanolate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride / 1,2-dimethoxyethane / Inert atmosphere

2: boron tribromide / dichloromethane / -78 - 20 °C

With boron tribromide; sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In 1,2-dimethoxyethane; dichloromethane; 1: Buchwald-Hartwig coupling;

Reference yield:

: 33440-72-1
2-(4-chlorobenzyl)-3-methylnaphthalene-1,4-dione

: 1189395-15-0
P_TM₈₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 20 °C

1.2: 60 °C

2.1: sodium t-butanolate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride / 1,2-dimethoxyethane / Inert atmosphere

3.1: boron tribromide / dichloromethane / -78 - 20 °C

With hydrogenchloride; boron tribromide; tin(ll) chloride; sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; 2.1: Buchwald-Hartwig coupling;