ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

Base Information

Chemical Name:ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate
CAS No.:1273583-74-6
Molecular Formula:C₂₄H₃₄N₂O₅
Molecular Weight:430.544
Hs Code.:

Synonyms:ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

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Chemical Property of ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

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Technology Process of ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

There total 3 articles about ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1273583-79-1
(E)-ethyl 4-((1-(butylcarbamoyl)cyclopentyl)(4-methoxybenzyl)amino)-4-oxobut-2-enoate

: 1273583-74-6
ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

Guidance literature:: In water; at 200 ℃; for 1h; under 13876.4 Torr; Microwave irradiation; Capped vial;
DOI:10.1021/jo102305q

Reference yield: 85.0%

: C₂₄H₃₄N₂O₅

: 1273583-74-6
ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

Guidance literature:: In water; at 200 ℃; for 1h; under 1125.11 Torr; Microwave irradiation;
DOI:10.1021/jo201525r

Reference yield:

: 3-ethoxycarbonylacrylic acid

: 2769-64-4
n-butyl isonitrile

: 2393-23-9
4-methoxy-benzylamine

: 120-92-3
cyclopentanone

: 1273583-74-6
ethyl 2-(9-butyl-6-(4-methoxybenzyl)-7,10-dioxo-6,9-diazaspiro[4.5]decan-8-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

2: water / 1 h / 200 °C / 1125.11 Torr / Microwave irradiation

In water; 1: Ugi four component coupling (U-4CC) / 2: 6-exo-trig aza-Michael reaction;
DOI:10.1021/jo201525r