(C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

Base Information

Chemical Name:(C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)
CAS No.:111507-06-3
Molecular Formula:C₂₂H₁₉O₂P
Molecular Weight:346.365
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)2PO<sub>2</sub>CC(CH<sub>3</sub>)CH(C<sub>6</sub>H<sub>5</sub>)

Synonyms:(C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

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Chemical Property of (C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

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Technology Process of (C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

There total 1 articles about (C₆H₅)2PO₂CC(CH₃)CH(C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1199-77-5
α-methylcinnamic acid

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 111507-06-3
(C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

Guidance literature:: With triethylamine; In tetrahydrofuran; at -20 ℃;

Reference yield: 70.0%

: di-μ-chloro-bis[bis(cyclo-octene)rhodium]

: 74839-84-2
(R,R)-chiraphos

: 111507-06-3
(C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

: (2R,3R)(+)-bis(diphenylphosphino)butane(diphenylphosphino E-2-methyl-3-phenylpropeonate)rhodium(I) hexafluorophosphate

Guidance literature:: With thallium(I) hexafluorophosphate; In tetrahydrofuran; Rh-Compd. and (+)-chiraphos stirred for 45 min, evapd. in vac., washed with light petroleum, dried in vac., residue dissolved, Ph2PO2CCMeCHPh in THF added, stirred for 30 min, TlF6 added, stirred for 40 min, filtered, soln. reduced in vac.; addn. of light petroleum , pptn., filtered, dried under vac.;
DOI:10.1039/DT9910001929

Reference yield:

: di-μ-chloro-bis[bis(cyclo-octene)rhodium]

: 111507-06-3
(C₆H₅)2PO₂CC(CH₃)CH(C₆H₅)

: (RhCl(C₆H₅)2PO₂CCCH₃CH(C₆H₅))2

Guidance literature:: In tetrahydrofuran; to a suspn. of Rh-complex in CH2Cl2 was added a soln. of Ph2PO2CCMeCHPh in THF; filtered, the solvent was removed by evapn. under reduced pressure, light petroleum was added quickly to this concd. soln. (crystn.); elem. anal.;