5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

Base Information

Chemical Name:5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene
CAS No.:83637-58-5
Molecular Formula:C₂₄H₂₆O₂S
Molecular Weight:378.535
Hs Code.:

Synonyms:5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

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Chemical Property of 5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

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Technology Process of 5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

There total 8 articles about 5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30267-36-8
5-methoxybenzocyclobuten-1-yl toluene-p-sulphonate

: 83637-58-5
5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 9 steps

1: dimethylformamide

2: m-chloroperbenzoic acid / CH₂Cl₂

3: 38 percent / lithium di-isopropylamide / tetrahydrofuran

4: pyridinium chlorochromate / CH₂Cl₂

5: zinc / acetic acid

6: 70 percent / H₂ / Pd/C / methanol

7: NaH / benzene

9: pyridine

With hydrogen; sodium hydride; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; zinc; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1039/c39820000699

Reference yield:

: 83637-50-7
5-methoxybenzocyclobut-1-enyl phenyl sulphide

: 83637-58-5
5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 8 steps

1: m-chloroperbenzoic acid / CH₂Cl₂

2: 38 percent / lithium di-isopropylamide / tetrahydrofuran

3: pyridinium chlorochromate / CH₂Cl₂

4: zinc / acetic acid

5: 70 percent / H₂ / Pd/C / methanol

6: NaH / benzene

8: pyridine

With hydrogen; sodium hydride; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; zinc; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; acetic acid; benzene;
DOI:10.1039/c39820000699

Reference yield:

: 83637-54-1
5-methoxy-1-(2-methyl-3-oxocyclohex-1-enylmethyl)-1,2-dihydrocyclobutabenzene

: 83637-58-5
5-methoxy-1-(2-methyl-3-oxo-4-phenylthiomethylenecyclohexylmethyl)-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / H₂ / Pd/C / methanol

2: NaH / benzene

4: pyridine

With hydrogen; sodium hydride; palladium on activated charcoal; In pyridine; methanol; benzene;
DOI:10.1039/c39820000699