N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine

Base Information

• Chemical Name: N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine
• CAS No.: 760952-86-1
• Molecular Formula: C₂₆H₂₆N₈
• Molecular Weight: 450.546
• Mol file: 760952-86-1.mol

Synonyms:N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine

Chemical Property of N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine

There total 2 articles about N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

pyridine-2-carbaldehyde (1121-60-4) + bis((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amine (760952-85-0) → N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine (760952-86-1)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;

DOI:10.1021/ja105743g

Reference yield: 83.0%

N,N-di-2-propyn-1-yl-2-pyridinemethanamine + benzyl azide (622-79-7) → N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine (760952-86-1)

Guidance literature:

With copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1007/s11243-014-9849-2

Reference yield: 85.0%

potassium hexafluorophosphate (17084-13-8) + N,N-bis[[1-(phenylmethyl)-1H-1,2,3-triazol-4-yl]methyl]-2-pyridinemethaneamine (760952-86-1) + Ru(bpy)(DMSO)2Cl2 → [Ru(L3)(2,2'-bipyridine)](PF6)2*1.1H2O

Guidance literature:

In 1,2-dimethoxyethane; at 150 ℃; Inert atmosphere;

DOI:10.1021/ic502807d

upstream raw materials:

pyridine-2-carbaldehyde

bis((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)amine

benzyl azide

Downstream raw materials:

C₂₈H₂₆FeN₁₀S₂