Technology Process of (1R,2S,6S,7R,8R)-4,4-Dimethyl-7-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-trityloxymethyl-tetrahydro-pyran-2-yloxy)-3,5,9,11-tetraoxa-tricyclo[6.2.1.02,6]undecane
There total 1 articles about (1R,2S,6S,7R,8R)-4,4-Dimethyl-7-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-trityloxymethyl-tetrahydro-pyran-2-yloxy)-3,5,9,11-tetraoxa-tricyclo[6.2.1.02,6]undecane which
guide to synthetic route it.
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synthetic route:
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130766-25-5
(1R,2S,6S,7R,8R)-4,4-Dimethyl-7-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-trityloxymethyl-tetrahydro-pyran-2-yloxy)-3,5,9,11-tetraoxa-tricyclo[6.2.1.02,6]undecane
- Guidance literature:
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With
tetra-(n-butyl)ammonium iodide; 2,6-lutidinium p-toluenesulfonate;
4 A molecular sieve;
In
toluene;
at 23 ℃;
for 55h;
Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)97729-3