sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

Base Information

Chemical Name:sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate
CAS No.:934221-61-1
Molecular Formula:C₂₉H₃₁N₂O₅*Na
Molecular Weight:510.565
Hs Code.:

Synonyms:sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

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Chemical Property of sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

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Technology Process of sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

There total 8 articles about sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 934221-59-7
N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosine methyl ester

: 934221-61-1
sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

Guidance literature:: With sodium hydroxide; In ethanol; chloroform; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2011.08.001

Reference yield:

: 60142-77-0
N-(N-benzoyl-L-phenylalanyl)-L-tyrosine methyl ester

: 934221-61-1
sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: sodium hydroxide / ethanol; chloroform / 2 h / 20 °C

With potassium carbonate; sodium hydroxide; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.001

Reference yield:

: 2566-22-5
N-benzoyl-L-phenylalanine

: 934221-61-1
sodium N-(N-benzoyl-L-phenylalanyl)-O-butyl-L-tyrosinate

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine; isobutyl chloroformate / dichloromethane / 1.5 h / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: sodium hydroxide / ethanol; chloroform / 2 h / 20 °C

With 4-methyl-morpholine; potassium carbonate; sodium hydroxide; isobutyl chloroformate; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.001