N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Base Information

• Chemical Name: N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole
• CAS No.: 155911-36-7
• Molecular Formula: C₈₆H₈₃N₅O₁₄
• Molecular Weight: 1410.63

Synonyms:N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Chemical Property of N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

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Technology Process of N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

There total 1 articles about N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

(1S,5R,7S)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carbonyl chloride (146651-53-8) + N-(4-(methoxycarbonyl)phenyl)-3,6-diaminocarbazole (155911-35-6) → N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole (155911-36-7)

Guidance literature:

With pyridine; for 2h; Ambient temperature;

DOI:10.1021/ja00087a013

Reference yield: 82.0%

N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole (155911-36-7) → N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((hydroxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Guidance literature:

With formic acid; hydrogen bromide; at 0 ℃; for 0.0833333h;

DOI:10.1021/ja00087a013

Reference yield: 78.0%

N-(4-(methoxycarbonyl)phenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole (155911-36-7) → N-(4-carboxyphenyl)-3,6-bis<((cis,cis-2,4-dioxo-1,5,7-tris((benzyloxy)methyl)-3-azabicyclo<3.3.1>non-7-yl)carbonyl)amino>carbazole

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; ethanol; for 20h; Ambient temperature;

DOI:10.1021/ja00087a013

upstream raw materials:

(1S,5R,7S)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carbonyl chloride

N-(4-(methoxycarbonyl)phenyl)-3,6-diaminocarbazole

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