C₃₂H₄₂N₆O₃S

Base Information

• Chemical Name: C₃₂H₄₂N₆O₃S
• CAS No.: 1190400-75-9
• Molecular Formula: C₃₂H₄₂N₆O₃S
• Molecular Weight: 590.79
• Mol file: 1190400-75-9.mol

Synonyms:C₃₂H₄₂N₆O₃S

Chemical Property of C₃₂H₄₂N₆O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₄₂N₆O₃S

There total 4 articles about C₃₂H₄₂N₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-2-(isopropylsulphonyl)benzene (76697-50-2) → C32H42N6O3S (1190400-75-9)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / water; isopropyl alcohol / 150 °C / Microwave irradiation

2: hydrogenchloride / water; isopropyl alcohol / 0.5 h / 160 °C / Microwave irradiation

3: triethylamine / N,N-dimethyl-formamide / 0.17 h / 100 °C / Microwave irradiation

With hydrogenchloride; triethylamine; In water; N,N-dimethyl-formamide; isopropyl alcohol;

DOI:10.1016/j.bmcl.2015.11.049

Reference yield:

C31H40N6O3S (1190399-88-2) + methyl iodide (74-88-4) → C32H42N6O3S (1190400-75-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 100 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1016/j.bmcl.2015.11.049

Reference yield:

C16H17ClN4O2S → C32H42N6O3S (1190400-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / water; isopropyl alcohol / 0.5 h / 160 °C / Microwave irradiation

2: triethylamine / N,N-dimethyl-formamide / 0.17 h / 100 °C / Microwave irradiation

With hydrogenchloride; triethylamine; In water; N,N-dimethyl-formamide; isopropyl alcohol;

DOI:10.1016/j.bmcl.2015.11.049

upstream raw materials:

2,4-dichloro-5-methyl-7H-pyrrolo[2,3-d]pyrimidine

1-amino-2-(isopropylsulphonyl)benzene

C₃₁H₄₀N₆O₃S

methyl iodide

Refernces