2-cyclohexyl-2-acetoxyacetaldehyde

Base Information

• Chemical Name: 2-cyclohexyl-2-acetoxyacetaldehyde
• CAS No.: 56697-99-5
• Molecular Formula: C₁₀H₁₆O₃
• Molecular Weight: 184.235
• Mol file: 56697-99-5.mol

Synonyms:2-cyclohexyl-2-acetoxyacetaldehyde

Chemical Property of 2-cyclohexyl-2-acetoxyacetaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-cyclohexyl-2-acetoxyacetaldehyde

There total 3 articles about 2-cyclohexyl-2-acetoxyacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(S)-1-cyclohexyl-2-propen-1-ol acetate (95124-06-4) → 2-cyclohexyl-2-acetoxyacetaldehyde (56697-99-5)

Guidance literature:

(S)-1-cyclohexyl-2-propen-1-ol acetate; With ozone; In dichloromethane; at -78 ℃;

With triphenylphosphine; In dichloromethane; at 20 ℃; for 4h; Further stages.;

DOI:10.1016/j.tet.2007.08.074

Reference yield:

1-cyclohexylprop-2-en-1-ol (4352-44-7) → 2-cyclohexyl-2-acetoxyacetaldehyde (56697-99-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: O₃ / CH₂Cl₂; methanol / -78 °C

1.2: Me₂S / methanol; CH₂Cl₂ / -78 °C

With ozone; In methanol; dichloromethane;

DOI:10.1021/ol990632u

Reference yield:

→ 2-cyclohexyl-2-acetoxyacetaldehyde (56697-99-5)

Guidance literature:

geschutzten Aldehyd;

upstream raw materials:

(S)-1-cyclohexyl-2-propen-1-ol acetate

1-cyclohexylprop-2-en-1-ol

Downstream raw materials:

5-cyclohexyl-5-hydrofuran-2-one

acetic acid 2-cyclohexyl-2-oxoethyl ester

(1,2-diacetoxyethyl)cyclohexane