(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

Base Information

Chemical Name:(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide
CAS No.:1330633-86-7
Molecular Formula:C₁₉H₂₁NO₆S
Molecular Weight:391.445
Hs Code.:

Synonyms:(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

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Chemical Property of (E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

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Technology Process of (E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

There total 8 articles about (E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 908344-21-8
3-nitro-4-methoxybenzyl mercaptan

: 136612-71-0
(2,4,6-Trimethoxyphenyl)acetylene

: 1330633-85-6
(Z)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

: 1330633-86-7
(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

Guidance literature:: With triethyl borane; In hexane; benzene; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm200570p

Reference yield:

: 1330633-87-8
2-(2’,2’-dibromovinyl)-1,3,5-trimethoxybenzene

: 1330633-86-7
(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C

2: triethyl borane / hexane; benzene / 2 h / 25 °C / Inert atmosphere

With n-butyllithium; triethyl borane; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/jm200570p

Reference yield:

: 3-nitro-4-methoxybenzylisothiouronium salt

: 1330633-86-7
(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / hexane / Inert atmosphere

2: triethyl borane / hexane; benzene / 2 h / 25 °C / Inert atmosphere

With triethyl borane; ammonia; In hexane; benzene;
DOI:10.1021/jm200570p