2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

Base Information

Chemical Name:2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester
CAS No.:906008-02-4
Molecular Formula:C₁₉H₂₁O₄P
Molecular Weight:344.347
Hs Code.:

2-phenyl-2,4,5,6-tetrahydro-cyclopenta[<i>c</i>]phosphole-1,3-dicarboxylic acid diethyl ester

Synonyms:2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

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Chemical Property of 2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

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Technology Process of 2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

There total 1 articles about 2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 34497-18-2
diethyl nona-2,7-diynedioate

: 644-97-3
Dichlorophenylphosphine

: 906008-02-4
2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

Guidance literature:: diethyl nona-2,7-diynedioate; With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -50 ℃;

Dichlorophenylphosphine; In diethyl ether; at -50 - 20 ℃;
DOI:10.1021/jo0605748

Reference yield: 63.0%

: 906008-02-4
2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

: 906008-08-0
2,5-bis(hydroxymethyl)-1-phenyl-1-thiophosphole

Guidance literature:: 2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester; With diisobutylaluminium hydride; In hexane; at -50 ℃; for 1h;

With sulfur; In hexane; at -50 - 20 ℃;
DOI:10.1021/jo0605748

Reference yield: 40.0%

: 906008-02-4
2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester

: 75-16-1
methylmagnesium bromide

: 2-[3-(1-hydroxy-1-methyl-ethyl)-2-phenyl-2-thioxo-2,4,5,6-tetrahydro-2λ⁵-cyclopenta[c]phosphol-1-yl]-propan-2-ol

Guidance literature:: 2-phenyl-2,4,5,6-tetrahydro-cyclopenta[c]phosphole-1,3-dicarboxylic acid diethyl ester; methylmagnesium bromide; In tetrahydrofuran; at -78 - 50 ℃;

With sulfur; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1021/jo0605748