cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin

Base Information

Chemical Name:cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin
CAS No.:180711-72-2
Molecular Formula:C₅₂H₄₄CoN₄O₈
Molecular Weight:911.937
Hs Code.:

Synonyms:cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin

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Technology Process of cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin

There total 2 articles about cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 5,10,15,20-tetrakis(2’,6’-dimethoxyphenyl)-21H,23H-porphyrin

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 180711-72-2
cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin

Guidance literature:: With 2,6-dimethylpyridine; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.ica.2020.119594

Reference yield:

: 3392-97-0
2,6-dimethoxybenzaldehyde

: 180711-72-2
cobalt(II)-5,10,15,20-tetrakis(2′,6′-dimethoxyphenyl)-21H,23H-porphyrin

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / chloroform / 1.5 h / 20 °C / Inert atmosphere; Darkness

1.2: 1.5 h / 65 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

With 2,6-dimethylpyridine; boron trifluoride diethyl etherate; In tetrahydrofuran; chloroform;
DOI:10.1016/j.ica.2020.119594