Technology Process of C40H62O4SSi
There total 7 articles about C40H62O4SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
tetrahydrofuran;
at -30 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene / 8 h / 60 °C
2: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / 0 °C
3: triphenylphosphine; carbon tetrabromide / dichloromethane / 0.5 h / 0 °C
4: potassium tert-butylate / tetrahydrofuran / 1 h / -30 °C
With
carbon tetrabromide; potassium tert-butylate; diisobutylaluminium hydride; triphenylphosphine;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: salicylic acid; tert.-butylhydroperoxide; selenium(IV) oxide / water / 0 - 4 °C
1.2: 2 h / 0 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 0 °C
3.1: potassium tert-butylate / tetrahydrofuran / 1 h / -30 °C
With
1H-imidazole; tert.-butylhydroperoxide; selenium(IV) oxide; potassium tert-butylate; salicylic acid;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;