S-tert-butyl 5-phenylpentathionate

Base Information

Chemical Name:S-tert-butyl 5-phenylpentathionate
CAS No.:114739-15-0
Molecular Formula:C₁₅H₂₂OS
Molecular Weight:250.405
Hs Code.:

Synonyms:S-tert-butyl 5-phenylpentathionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-tert-butyl 5-phenylpentathionate

Chemical Property:

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Technology Process of S-tert-butyl 5-phenylpentathionate

There total 3 articles about S-tert-butyl 5-phenylpentathionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: S-tert-Butyl 5-phenylpent-2-enethioate

: 114739-15-0
S-tert-butyl 5-phenylpentathionate

Guidance literature:: With copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol; In toluene; at 20 ℃; for 12h; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c1ob05352c

Reference yield:

: 24271-22-5,55320-96-2,138034-94-3
5-phenyl-2(E)-pentenoic acid

: 114739-15-0
S-tert-butyl 5-phenylpentathionate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 1 h / Inert atmosphere

2: zinc / toluene / 1 h / 20 °C / Inert atmosphere

3: copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol / toluene / 12 h / 20 °C / Inert atmosphere

With oxalyl dichloride; copper acetate monohydrate; o-phenylenebis(diphenylphosphine); N,N-dimethyl-formamide; zinc; tert-butyl alcohol; In tetrahydrofuran; toluene;
DOI:10.1039/c1ob05352c

Reference yield:

: 485809-19-6
5-phenyl-2-pentenoic acid chloride

: 114739-15-0
S-tert-butyl 5-phenylpentathionate

Guidance literature:: Multi-step reaction with 2 steps

1: zinc / toluene / 1 h / 20 °C / Inert atmosphere

2: copper acetate monohydrate; o-phenylenebis(diphenylphosphine); tert-butyl alcohol / toluene / 12 h / 20 °C / Inert atmosphere

With copper acetate monohydrate; o-phenylenebis(diphenylphosphine); zinc; tert-butyl alcohol; In toluene;
DOI:10.1039/c1ob05352c