N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

Base Information

Chemical Name:N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide
CAS No.:1026133-26-5
Molecular Formula:C₂₃H₂₈F₃NO₄
Molecular Weight:439.475
Hs Code.:

<i>N</i>-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

Synonyms:N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

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Chemical Property of N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

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Technology Process of N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

There total 3 articles about N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 289889-53-8
(+/-)-N-trifluoroacetyl-1-[2,5-dimethoxy-4-(3-(4-methoxy)phenylpropionyl)phenyl]-2-aminopropane

: 1026133-26-5
N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

Guidance literature:: With perchloric acid; hydrogen; acetic acid; palladium on activated charcoal; for 6h; under 3102.89 Torr;
DOI:10.1021/jm9906062

Reference yield:

: 15893-42-2
3-(4-methoxyphenyl)propionyl chloride

: 1026133-26-5
N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / TiCl₄ / CH₂Cl₂ / 0.5 h / -30 °C

2: H₂; AcOH; 70 percent HClO₄ / 10 percent Pd/C / 6 h / 3102.89 Torr

With perchloric acid; hydrogen; titanium tetrachloride; acetic acid; palladium on activated charcoal; In dichloromethane; 1: Friedel-Crafts acylation / 2: Reduction;
DOI:10.1021/jm9906062

Reference yield:

: 79315-43-8
(+/-)-N-[2-(2,5-dimethoxyphenyl)-1-methylethyl]-2,2,2-trifluoroacetamide

: 1026133-26-5
N-(2-{2,5-dimethoxy-4-[3-(4-methoxy-phenyl)-propyl]-phenyl}-1-methyl-ethyl)-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / TiCl₄ / CH₂Cl₂ / 0.5 h / -30 °C

2: H₂; AcOH; 70 percent HClO₄ / 10 percent Pd/C / 6 h / 3102.89 Torr

With perchloric acid; hydrogen; titanium tetrachloride; acetic acid; palladium on activated charcoal; In dichloromethane; 1: Friedel-Crafts acylation / 2: Reduction;
DOI:10.1021/jm9906062