2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

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Chemical Name:2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester
CAS No.:91622-14-9
Molecular Formula:C₃₂H₃₂ClN₃O₄S
Molecular Weight:590.143
Hs Code.:

Synonyms:2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

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Chemical Property of 2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

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Technology Process of 2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

There total 1 articles about 2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68672-66-2
(Z)-2-(1-t-butoxycarbonyl-1-methylethoxyimino)-2-[2-(triphenylmethylamino)thiazol-4-yl]acetic acid

: 91622-14-9
2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1039/b007286i

Reference yield: 35.0%

: C₂₂H₂₁N₃O₄S

: 91622-14-9
2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

: C₅₄H₅₂N₆O₈S₂

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)97262-9

Reference yield:

: (S)-6-amino-2-(((1,5-dihydroxy-4-oxo-1,4-dihydropyridin-2-yl)methyl)carbamoyl)-5-oxo-6,7-dihydro-1H,5H-pyrazolo[1,2-a]pyrazole-3-carboxylic acid trifluoroacetate

: 91622-14-9
2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

: (S,Z)-6-(2-(((1-(tert-butoxy)-2-methyl-1-oxopropan-2-yl)oxy)imino)-2-(2-(tritylamino)thiazol-4-yl)acetamido)-2-(((1,5-dihydroxy-4-oxo-1,4-dihydropyridin-2-yl)methyl)carbamoyl)-5-oxo-6,7-dihydro-1H,5H-pyrazolo[1,2-a]pyrazole-3-carboxylic acid

Guidance literature:: (S)-6-amino-2-(((1,5-dihydroxy-4-oxo-1,4-dihydropyridin-2-yl)methyl)carbamoyl)-5-oxo-6,7-dihydro-1H,5H-pyrazolo[1,2-a]pyrazole-3-carboxylic acid trifluoroacetate; With N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; N-ethyl-N,N-diisopropylamine; In acetonitrile; for 1h; Cooling with ice;

2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester; In acetonitrile; at 20 ℃; for 1.5h;