Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

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Chemical Name:Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate
CAS No.:142466-85-1
Molecular Formula:C₃₇H₃₈N₅O₁₀S₂*K
Molecular Weight:815.967
Hs Code.:

Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

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Chemical Property of Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

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Technology Process of Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

There total 2 articles about Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142488-27-5
Potassium; (2S,3S)-3-benzyloxycarbonylamino-2-benzyloxycarbonylmethyl-4-oxo-azetidine-1-sulfonate

: 142466-85-1
Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / H₂ / 10percent Pd/C / dimethylformamide / 1.5 h / Ambient temperature

2: 1.) BSA / 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, a) -45 deg C, 15 min, b) RT, 1 h

With benzenesulfonamide; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(92)90101-6

Reference yield:

: 91622-14-9
2-[1-Chlorocarbonyl-1-[2-(trityl-amino)-thiazol-4-yl]-meth-(Z)-ylideneaminooxy]-2-methyl-propionic acid tert-butyl ester

: 142466-84-0
Potassium; (2S,3S)-3-amino-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

: 142466-85-1
Potassium; (2S,3S)-3-{2-[(Z)-1-tert-butoxycarbonyl-1-methyl-ethoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-carboxymethyl-4-oxo-azetidine-1-sulfonate

Guidance literature:: With benzenesulfonamide; Yield given. Multistep reaction; 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, a) -45 deg C, 15 min, b) RT, 1 h;
DOI:10.1016/0223-5234(92)90101-6