1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Base Information

• Chemical Name: 1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol
• CAS No.: 908853-73-6
• Molecular Formula: C₅₉H₆₄O₁₂
• Molecular Weight: 965.15

Synonyms:1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Chemical Property of 1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Chemical Property:

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MSDS Files:

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Technology Process of 1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

There total 1 articles about 1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl trichloroacetimidate (108869-64-3,130177-78-5,129163-12-8) + 1-O-allyl-3,4,5-tri-O-benzyl-D-myo-inositol (202845-42-9) → 1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol (908853-73-6) + 1-O-allyl-2,6-di-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol (908853-78-1)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -40 - 0 ℃; for 1.16667h;

DOI:10.1016/j.bmc.2006.04.037

Reference yield: 95.0%

1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol (908853-73-6) → 1-O-allyl-3,4,5-tri-O-benzyl-6-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol (909026-35-3)

Guidance literature:

With sodium methylate; In methanol; for 3h;

DOI:10.1016/j.bmc.2006.04.037

Reference yield: 65.0%

1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol (908853-73-6) + benzoyl chloride (98-88-4) → 1-O-allyl-6-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2-O-benzoyl-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:

With pyridine; for 8h;

DOI:10.1016/j.bmc.2006.04.037

upstream raw materials:

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl trichloroacetimidate

1-O-allyl-3,4,5-tri-O-benzyl-D-myo-inositol

Downstream raw materials:

1-O-allyl-3,4,5-tri-O-benzyl-6-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

2,3,4,5-tetra-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

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