3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

Base Information

Chemical Name:3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole
CAS No.:1318779-45-1
Molecular Formula:C₂₃H₂₅NO₃
Molecular Weight:363.456
Hs Code.:

Synonyms:3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

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Chemical Property of 3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

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Technology Process of 3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

There total 4 articles about 3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 3-(ethoxycarbonyl)-2-methyl-5-(1'-phenylvinyl)-4,5-dihydrofuran

: 104-94-9
4-methoxy-aniline

: 1318779-45-1
3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In toluene; at 90 ℃; for 10h; Inert atmosphere;
DOI:10.1002/adsc.201100002

Reference yield: 72.0%

: 591-50-4
iodobenzene

: 114707-16-3
ethyl 2-(buta-2,3-dienyl)-3-oxobutanoate

: 104-94-9
4-methoxy-aniline

: 1318779-45-1
3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In toluene; at 90 ℃; for 10h; Inert atmosphere;
DOI:10.1002/adsc.201100002

Reference yield: 49.0%

: 591-50-4
iodobenzene

: 114707-16-3
ethyl 2-(buta-2,3-dienyl)-3-oxobutanoate

: 104-94-9
4-methoxy-aniline

: 1318779-70-2
C₁₇H₂₁NO₃

: 1318779-45-1
3-(ethoxycarbonyl)-1-(4-methoxyphenyl)-2-methyl-5-(1-phenylvinyl)-4,5-dihydro-1H-pyrrole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In toluene; at 90 ℃; for 1.16667h; Inert atmosphere;
DOI:10.1002/adsc.201100002