Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

Base Information

Chemical Name:Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester
CAS No.:911829-46-4
Molecular Formula:C₁₀H₂₀O₆S₂
Molecular Weight:300.397
Hs Code.:

Synonyms:Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

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Chemical Property of Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

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Technology Process of Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

There total 1 articles about Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1792-81-0
cis-1,2-cyclohexane

: 6378-11-6
ethyl chlorosulfite

: 911829-46-4
Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

Guidance literature:: With pyridine; In ethyl acetate; at 0 ℃;
DOI:10.1021/jo060404v

Reference yield: 93.0%

: 911829-46-4
Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

: 911829-53-3
Sulfuric acid (1R,2S)-2-ethoxysulfonyloxy-cyclohexyl ester ethyl ester

Guidance literature:: With sodium periodate; ruthenium trichloride; In methanol; dichloromethane; water; for 1h;
DOI:10.1021/jo060404v

Reference yield:

: 911829-46-4
Sulfurous acid (1R,2S)-2-ethoxysulfinyloxy-cyclohexyl ester ethyl ester

: cis-cyclohexane-1,2-diol 1,2-disulfate disodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaIO₄ / RuCl₃ / CH₂Cl₂; methanol; H₂O / 1 h

2: 99 percent / NaI / acetone / 20 °C

With sodium periodate; sodium iodide; ruthenium trichloride; In methanol; dichloromethane; water; acetone;
DOI:10.1021/jo060404v