4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

Base Information

Chemical Name:4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide
CAS No.:1346665-43-7
Molecular Formula:C₂₅H₂₄ClN₃O₅S
Molecular Weight:514.002
Hs Code.:

Synonyms:4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

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Chemical Property of 4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

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Technology Process of 4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

There total 4 articles about 4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346665-30-2
C₁₃H₈BrClN₂O₃

: 871333-00-5
C₁₂H₁₈BNO₄S

: 1346665-43-7
4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; water; at 80 ℃; for 3h; Inert atmosphere;

Reference yield:

: 53324-38-2
4-bromo-3-nitroaniline

: 1346665-43-7
4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; ethanol; water / 3 h / 80 °C / Inert atmosphere

With dmap; sodium carbonate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; dichloromethane; water;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 1346665-43-7
4-chloro-N-(2'-methyl-2-nitro-5'-(piperidin-1-ylsulfonyl)-[1,1'-biphenyl]-4-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; ethanol; water / 3 h / 80 °C / Inert atmosphere

With dmap; sodium carbonate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; dichloromethane; water;