tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

Base Information

• Chemical Name: tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate
• CAS No.: 1187451-02-0
• Molecular Formula: C₂₉H₃₅BrN₄O₆S
• Molecular Weight: 647.59

Synonyms:tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

Chemical Property of tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

Chemical Property:

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Technology Process of tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

There total 8 articles about tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl (tert-butoxycarbonyl(6-(hydroxymethyl)pyridin-2-yl)amino)acetate (1187450-49-2) + N-(4-bromobenzyl)pyridin-2-ylsulfonamide (1313217-74-1) → tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate (1187451-02-0)

Guidance literature:

With tributylphosphine; diamide; In tetrahydrofuran; at 20 ℃; for 13h;

Reference yield: 100.0%

→ tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate (1187451-02-0)

Guidance literature:

Reference yield: 91.0%

tert-butyl (tert-butoxycarbonyl{6-[(pyridin-2-ylsulfonyl)aminomethyl]pyridin-2-yl}amino)acetate (1187450-89-0) + 1-bromomethyl-4-bromobenzene (589-15-1) → tert-butyl (tert-butoxycarbonyl{6-[(4-bromobenzyl)(pyridin-2-yl-sulfonyl)aminomethyl]pyridin-2-yl}amino)acetate (1187451-02-0)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 16h;

upstream raw materials:

tert-butyl (tert-butoxycarbonyl{6-[(pyridin-2-ylsulfonyl)aminomethyl]pyridin-2-yl}amino)acetate

1-bromomethyl-4-bromobenzene

pyridine-2-sulfonyl chloride

bromoacetic acid tert-butyl ester

Downstream raw materials:

tert-butyl [tert-butoxycarbonyl(6-{(pyridin-2-ylsulfonyl)[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzyl]aminomethyl}pyridin-2-yl)amino]acetate

tert-butyl [tert-butoxycarbonyl(6-{[4-(phenylamino)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

tert-butyl [tert-butoxycarbonyl(6-{[4-(1-methyl-1-pentenyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-yl)amino]acetate

(6-{[4-(1-methyl-1-pentenyl)benzyl](pyridin-2-ylsulfonyl)aminomethyl}pyridin-2-ylamino)acetic acid

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