N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Base Information

Chemical Name:N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide
CAS No.:1201663-61-7
Molecular Formula:C₂₈H₂₄Cl₂F₂N₂O₂S
Molecular Weight:561.48
Hs Code.:

Synonyms:N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Suppliers and Price of N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

There total 5 articles about N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1201663-60-6
3-(aminomethyl)-N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)benzenesulfonamide

: 459-57-4
4-fluorobenzaldehyde

: 1201663-61-7
N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Guidance literature:: 3-(aminomethyl)-N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)benzenesulfonamide; 4-fluorobenzaldehyde; In dichloromethane; at 20 ℃; for 1h;

With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; water; for 0.333333h;

Reference yield:

: 10203-08-4
3,5-dichlorobenzaldehyde

: 1201663-61-7
N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane; isopropyl alcohol / 1 h / 20 °C

1.2: 22 h / 20 °C / Inert atmosphere

1.3: 0.2 h

2.1: triethylamine / tetrahydrofuran / 17 h / 20 °C

3.1: diborane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.2: 0.5 h

4.1: dichloromethane / 1 h / 20 °C

4.2: 20 h / 20 °C / Inert atmosphere

4.3: 0.33 h

With triethylamine; diborane; In tetrahydrofuran; dichloromethane; isopropyl alcohol;

Reference yield:

: 1179959-12-6
N-(3,5-dichlorobenzyl)-1-(4-fluorophenyl)methanamine

: 1201663-61-7
N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 17 h / 20 °C

2.1: diborane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 0.5 h

3.1: dichloromethane / 1 h / 20 °C

3.2: 20 h / 20 °C / Inert atmosphere

3.3: 0.33 h

With triethylamine; diborane; In tetrahydrofuran; dichloromethane;