3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Base Information

Chemical Name:3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide
CAS No.:1201661-34-8
Molecular Formula:C₃₄H₂₆Cl₄F₂N₂O₅S₂
Molecular Weight:786.532
Hs Code.:

Synonyms:3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Suppliers and Price of 3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

There total 6 articles about 3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1201663-61-7
N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)-3-((4-fluorobenzylamino)methyl)benzenesulfonamide

: 23378-88-3
3,5-dichloro-2-hydroxybenzenesulfonyl chloride

: 1201661-34-8
3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 3.5h;

Reference yield:

: 1201663-60-6
3-(aminomethyl)-N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)benzenesulfonamide

: 1201661-34-8
3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 1 h / 20 °C

1.2: 20 h / 20 °C / Inert atmosphere

1.3: 0.33 h

2.1: triethylamine / tetrahydrofuran / 3.5 h / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 10203-08-4
3,5-dichlorobenzaldehyde

: 1201661-34-8
3,5-dichloro-N-(3-(N-(3,5-dichlorobenzyl)-N-(4-fluorobenzyl)sulfamoyl)benzyl)-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane; isopropyl alcohol / 1 h / 20 °C

1.2: 22 h / 20 °C / Inert atmosphere

1.3: 0.2 h

2.1: triethylamine / tetrahydrofuran / 17 h / 20 °C

3.1: diborane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.2: 0.5 h

4.1: dichloromethane / 1 h / 20 °C

4.2: 20 h / 20 °C / Inert atmosphere

4.3: 0.33 h

5.1: triethylamine / tetrahydrofuran / 3.5 h / 20 °C

With triethylamine; diborane; In tetrahydrofuran; dichloromethane; isopropyl alcohol;