1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

Base Information

Chemical Name:1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine
CAS No.:126811-34-5
Molecular Formula:C₁₈H₂₆N₂O
Molecular Weight:286.417
Hs Code.:

Synonyms:1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

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Technology Process of 1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

There total 1 articles about 1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 88056-92-2
(-)-2-cyano-6-phenyloxazolopiperidine

: 126811-34-5
1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

Guidance literature:: In diethyl ether; at -78 - 0 ℃;
DOI:10.1016/S0040-4039(01)93468-9

Reference yield: 91.0%

: 126811-34-5
1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

: (R)-2-[(S)-2-(1-Amino-pentyl)-piperidin-1-yl]-2-phenyl-ethanol

Guidance literature:: With sodium tetrahydroborate; In methanol;
DOI:10.1016/S0040-4039(01)93468-9

Reference yield:

: 126811-34-5
1-((3R,5S,8aR)-3-Phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-pentylideneamine

: 126811-37-8
N-[(R)-1-((S)-1-Benzoyl-piperidin-2-yl)-pentyl]-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / NaBH₄ / methanol

2: Pd(OH)2/C / methanol / 5 h

3: pyridine

With pyridine; sodium tetrahydroborate; palladium dihydroxide; In methanol;
DOI:10.1016/S0040-4039(01)93468-9