C₁₅H₂₁NO₃S

Base Information

Chemical Name:C₁₅H₂₁NO₃S
CAS No.:1268630-87-0
Molecular Formula:C₁₅H₂₁NO₃S
Molecular Weight:295.403
Hs Code.:

C<sub>15</sub>H<sub>21</sub>NO<sub>3</sub>S

Synonyms:C₁₅H₂₁NO₃S

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Chemical Property of C₁₅H₂₁NO₃S

Chemical Property:

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Technology Process of C₁₅H₂₁NO₃S

There total 4 articles about C₁₅H₂₁NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1268630-78-9
(Z)-N-(2-hydroxy-2-methylpropyl)-N-(4-hydroxybut-2-en-1-yl)-4-methylbenzenesulfonamide

: 1268630-87-0
C₁₅H₂₁NO₃S

Guidance literature:: With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dimethylsulfide gold(I) chloride; silver(I) triflimide; In dichloromethane; toluene; at -10 ℃; for 4h; optical yield given as %ee; Inert atmosphere; Darkness;
DOI:10.1002/chem.201002606

Reference yield:

: 1268631-13-5
C₂₁H₃₇NO₄SSi

: 1268630-87-0
C₁₅H₂₁NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

2: (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dimethylsulfide gold(I) chloride; silver(I) triflimide / dichloromethane; toluene / 4 h / -10 °C / Inert atmosphere; Darkness

With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dimethylsulfide gold(I) chloride; tetrabutyl ammonium fluoride; silver(I) triflimide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/chem.201002606

Reference yield:

: 29668-57-3
N-(2-hydroxy-2-methylpropyl)-4-methylbenzenesulfonamide

: 1268630-87-0
C₁₅H₂₁NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C / Inert atmosphere

1.2: 16 h / Inert atmosphere; Reflux

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

3.1: (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dimethylsulfide gold(I) chloride; silver(I) triflimide / dichloromethane; toluene / 4 h / -10 °C / Inert atmosphere; Darkness

With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dimethylsulfide gold(I) chloride; tetrabutyl ammonium fluoride; sodium hydride; silver(I) triflimide; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1002/chem.201002606