bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ²N,O¹]palladium(II)

Base Information

• Chemical Name: bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ²N,O¹]palladium(II)
• CAS No.: 1448531-22-3
• Molecular Formula: C₃₈H₄₀Br₄N₂O₂Pd
• Molecular Weight: 982.784
• Mol file: 1448531-22-3.mol

Synonyms:bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ²N,O¹]palladium(II)

Chemical Property of bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ²N,O¹]palladium(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ²N,O¹]palladium(II)

There total 2 articles about bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ²N,O¹]palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

sodium tetrachloropalladate(II) + 2-[(2,6-diisopropylphenyl)imino]methyl-4,6-dibromophenole (210882-81-8) → bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ2N,O1]palladium(II) (1448531-22-3)

Guidance literature:

In methanol; at 20 ℃; for 5h;

DOI:10.1007/s11243-013-9691-y

Reference yield: 73.0%

2-[(2,6-diisopropylphenyl)imino]methyl-4,6-dibromophenole (210882-81-8) + palladium diacetate (3375-31-3) → bis[2,4-dibromo-6-[(2,6-diisopropylphenyl)iminomethyl]phenolato-κ2N,O1]palladium(II) (1448531-22-3)

Guidance literature:

In ethanol; for 2h; Reflux; Inert atmosphere; Schlenk technique;

DOI:10.1007/s00706-017-2119-1

upstream raw materials:

2-[(2,6-diisopropylphenyl)imino]methyl-4,6-dibromophenole

palladium diacetate