4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

Base Information

Chemical Name:4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide
CAS No.:1312698-78-4
Molecular Formula:C₁₀H₁₁N₅OS₂
Molecular Weight:281.362
Hs Code.:

Synonyms:4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

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Chemical Property of 4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

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Technology Process of 4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

There total 4 articles about 4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-34-4
methylhydrazine

: 5-(4-isothiocyanatophenyl)-1,3,4-oxadiazole-2-thiol

: 1312698-78-4
4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

Guidance literature:: In water; toluene; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1312698-78-4
4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / 1 h / Reflux

2.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

2.2: pH 4

3.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

4.1: water; toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 5351-17-7
4-aminobenzohydrazide

: 1312698-78-4
4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)-1-methylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

1.2: pH 4

2.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

3.1: water; toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017