C₂₉H₂₈N₆O₄

Base Information

Chemical Name:C₂₉H₂₈N₆O₄
CAS No.:1466565-64-9
Molecular Formula:C₂₉H₂₈N₆O₄
Molecular Weight:524.579
Hs Code.:

C<sub>29</sub>H<sub>28</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₂₉H₂₈N₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₈N₆O₄

Chemical Property:

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Technology Process of C₂₉H₂₈N₆O₄

There total 2 articles about C₂₉H₂₈N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1466563-96-1
C₂₉H₂₇ClN₆O₄

: 73183-34-3
bis(pinacol)diborane

: 1466565-62-7
C₃₅H₃₉BN₆O₆

: 1466565-64-9
C₂₉H₂₈N₆O₄

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium acetate; XPhos; In 1,4-dioxane; at 110 ℃; for 8h; Inert atmosphere;

Reference yield:

: 21327-86-6
2-chloro-6-methylbenzoic acid

: 1466565-62-7
C₃₅H₃₉BN₆O₆

: 1466565-64-9
C₂₉H₂₈N₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 20 °C

1.2: 2 h / 25 - 40 °C / Cooling with ice

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere

2.2: 2 h / -30 - -10 °C / Inert atmosphere

2.3: 10.5 h / 20 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

4.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; potassium acetate / 1,4-dioxane / 8 h / 110 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; potassium acetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; XPhos; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide;