Technology Process of (+/-)-1,5,6-tri-O-benzyl-2,3-O-isopropylidene-4-O-p-methoxybenzyl-myo-inositol
There total 8 articles about (+/-)-1,5,6-tri-O-benzyl-2,3-O-isopropylidene-4-O-p-methoxybenzyl-myo-inositol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / dimethylformamide
2: toluene-p-sulphonic acid / acetone; H2O / 0.83 h / 20 °C
3: 64 percent / dibutyltin oxide, tetrabutylammonium bromide, molecular sieve 3 Angstroem / acetonitrile / Heating
4: 90 percent / sodium hydride / dimethylformamide
With
3 A molecular sieve; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/0008-6215(90)80132-M
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / dimethylformamide
2: toluene-p-sulphonic acid / acetone; H2O / 0.83 h / 20 °C
3: 64 percent / dibutyltin oxide, tetrabutylammonium bromide, molecular sieve 3 Angstroem / acetonitrile / Heating
4: 90 percent / sodium hydride / dimethylformamide
With
3 A molecular sieve; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/0008-6215(90)80132-M
