C₁₉H₂₂INO₃

Base Information

Chemical Name:C₁₉H₂₂INO₃
CAS No.:1266568-82-4
Molecular Formula:C₁₉H₂₂INO₃
Molecular Weight:439.293
Hs Code.:

C<sub>19</sub>H<sub>22</sub>INO<sub>3</sub>

Synonyms:C₁₉H₂₂INO₃

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Chemical Property of C₁₉H₂₂INO₃

Chemical Property:

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Technology Process of C₁₉H₂₂INO₃

There total 1 articles about C₁₉H₂₂INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1038778-89-0
(2-iodo-5-methoxyphenyl)carbamic acid 1,1-dimethylethyl ester

: 100-39-0
benzyl bromide

: 1266568-82-4
C₁₉H₂₂INO₃

Guidance literature:: (2-iodo-5-methoxyphenyl)carbamic acid 1,1-dimethylethyl ester; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201002287

Reference yield:

: 1266568-82-4
C₁₉H₂₂INO₃

: 1266568-73-3
C₂₄H₃₀N₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrabutylammomium bromide; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 20 - 100 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.67 h / -78 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

4.2: -40 - 0 °C / Inert atmosphere

5.1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

5.2: 0.17 h / 0 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 - 80 °C / Inert atmosphere

8.1: water; triphenylphosphine / tetrahydrofuran / 20 - 50 °C / Inert atmosphere

9.1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

10.1: water; potassium hydroxide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

With pyridine; dmap; sodium azide; tetrabutylammomium bromide; water; palladium diacetate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Heck reaction / 4.2: Wittig reaction;
DOI:10.1002/chem.201002287

Reference yield:

: 1266568-82-4
C₁₉H₂₂INO₃

: 1266568-74-4
C₂₅H₂₉ClN₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrabutylammomium bromide; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 20 - 100 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.67 h / -78 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

4.2: -40 - 0 °C / Inert atmosphere

5.1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

5.2: 0.17 h / 0 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 - 80 °C / Inert atmosphere

8.1: water; triphenylphosphine / tetrahydrofuran / 20 - 50 °C / Inert atmosphere

9.1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

10.1: water; potassium hydroxide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

11.1: pyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

With pyridine; dmap; sodium azide; tetrabutylammomium bromide; water; palladium diacetate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Heck reaction / 4.2: Wittig reaction;
DOI:10.1002/chem.201002287